TMSOTf distillation

Preparing the distillation

Assembling and drying the apparatus

Attach water inlet and outlet properly

Add TMSOTf to the flask under nitrogen using a glass funnel

Comment on the quality of the starting TMSOTf

Starting the distillation

Start distillation by adjusting pressure and raising temperature

First distillate observed

Safely interrupting the distillation when finished

Cannulation

Final product

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